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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2010 - Issue 1
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Original Articles

A Green Procedure for the Oxidation of Benzyl Halides to Aromatic Aldehydes or Ketones in Aqueous Media

Pengwu Zheng School of Pharmacy, Jiangxi Science and Technology Normal University, Nanchang, P. R. ChinaCorrespondence[email protected]
,
Li Yan School of Pharmacy, Jiangxi Science and Technology Normal University, Nanchang, P. R. China
,
Xiujie Ji School of Material Science and Engineering, Tianjin Polytechnic University, Tianjin, P. R. China
&
Xuemin Duan School of Pharmacy, Jiangxi Science and Technology Normal University, Nanchang, P. R. China
Pages 16-19 | Received 23 Apr 2009, Published online: 14 Dec 2010
 
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Abstract

Green oxidation of benzyl halides to the corresponding aldehydes or ketones was achieved in aqueous media using trimethylamine N-oxide generated in situ from trimethylamine and H2O2. The yield of the reaction was excellent and the workup was simple.

ACKNOWLEDGMENTS

This work was supported by the Science Funds of the Education Office of Jiangxi, China (granted No. [2006] 246 and [2007] 414) and by the Science Funds of Jiangxi Provincial Department of Science and Technology, China (granted No.[2005] 224).

Notes

a Isolated yield after column chromatography on SiO2.

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