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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 19
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Original Articles

Highly Efficient Synthesis of 3,5-Diaryl-1,2,4-thiadiazoles in Water–Wet Paste Conditions

Pages 2932-2938 | Received 09 Jun 2010, Published online: 29 Jun 2011
 

Abstract

1,3-Dibromo-5,5-diphenylimidazolidine-2,4-dione (N,N’-dibromo phenytoin) was efficiently used for the rapid conversion of thiobenzamides to the corresponding 3,5-diaryl-1,2,4-thiadiazoles in water–wet paste conditions.

Supplemental materials are available for this article. Go to the publisher's online edition of Synthetic Communications® to view the free supplemental file.

ACKNOWLEDGMENT

We are grateful to the University of Isfahan Research Council for financial support of this work.

Notes

a All products were characterized by 1H NMR, 13C NMR, and elemental analysis.

b All yields refer to pure isolated products.

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