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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 22
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Original Articles

Application of Wittig Reaction in Synthesis of Novel Pyridine Dicarboxylic Acid Derivatives with High Ligand Activity

Guo-Liang Gu Department of Chemical Engineering, Nanjing University of Science and Technology, Nanjing, ChinaCorrespondence[email protected]
,
Ming Lu Department of Chemical Engineering, Nanjing University of Science and Technology, Nanjing, China
&
Rui-Ren Tang School of Chemistry and Chemical Engineering, Central South University, Changsha, China
Pages 3403-3408 | Received 12 Nov 2009, Published online: 26 Jul 2011
 
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Abstract

A series of novel conjugated molecules with two pyridine dicarboxylic acid units have been synthesized by a Wittig reaction of corresponding alkyltriphenylphosphonium salts with aromatic aldehydes. The novel pyridine dicarboxylic acid derivatives with high ligand activity were completely characterized from their mass and 1H NMR spectra. The E-configuration of these alkenes was confirmed by infrared spectroscopic data.

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