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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 44, 2014 - Issue 23
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Original Articles

A Concise Synthesis of 3,5-Dicyano-6-trifluoromethylpyridine and Preparation of a Mono Thioamide

Pages 3456-3460 | Received 14 Jul 2014, Published online: 10 Oct 2014
 

Abstract

A concise 3-step synthesis of 3,5-dicyano-6-trifluoromethyl pyridine is reported from commercially available starting materials. Selective conversion of one cyano group into a thioamide offers further scope for derivatization.

GRAPHICAL ABSTRACT

ACKNOWLEDGMENTS

We acknowledge the experimental skills of Audrey Le Gall, Nicolas Held, and Michael Frühauf, together with the analytical skills of Leonhard Hagmann.

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