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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 45, 2015 - Issue 13
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Original Articles

Chlorination of Calix[4]arene Derivatives

E. A. IvanovaDepartment of Technology for Organic Synthesis, Ural Federal University, Yekaterinburg, Russia
,
P. E. ProkhorovaDepartment of Technology for Organic Synthesis, Ural Federal University, Yekaterinburg, Russia
,
V. V. MitinDepartment of Technology for Organic Synthesis, Ural Federal University, Yekaterinburg, Russia
,
T. V. GlukharevaDepartment of Technology for Organic Synthesis, Ural Federal University, Yekaterinburg, Russia
&
Yu. Yu. MorzherinDepartment of Technology for Organic Synthesis, Ural Federal University, Yekaterinburg, RussiaCorrespondence[email protected]
Pages 1592-1597 | Received 25 Feb 2015, Published online: 08 May 2015
 
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Abstract

New convenient method for synthesis of p-chlorinated calix[4]arenes is reported. The sulfuryl chloride was used for chlorination of unsubstituted at the lower rim calix[4]arenes. The products of this reaction were very suitable for further O-alkylation.

GRAPHICAL ABSTRACT

SUPPLEMENTAL MATERIAL

Full experimental details and1H and13C NMR spectra for this article can be accessed on the publisher’s website.

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