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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 45, 2015 - Issue 16
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Original Articles

Synthesis and Cation Recognition Study of Novel Benzo Crown Ether Functionalized Enamine Derivatives

Dayanand R. PatilDepartment of Chemistry, Shivaji University, Vidyanagar, Kolhapur, India
,
Dattatraya R. ChandamDepartment of Chemistry, Shivaji University, Vidyanagar, Kolhapur, India
,
Abhijeet G. MulikDepartment of Chemistry, Shivaji University, Vidyanagar, Kolhapur, India
,
Suryabala D. JagdaleDepartment of Chemistry, Shivaji University, Vidyanagar, Kolhapur, India
,
Prasad P. PatilDepartment of Chemistry, Shivaji University, Vidyanagar, Kolhapur, India;Department of Agrochemicals and Pest Management, Shivaji University, Vidyanagar, Kolhapur, India
&
Madhukar B. DeshmukhDepartment of Chemistry, Shivaji University, Vidyanagar, Kolhapur, IndiaCorrespondence[email protected]
Pages 1902-1911 | Received 26 Jan 2015, Published online: 20 Jul 2015
 
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Abstract

A novel series of benzo crown ether (dibenzo 18-crown-6 ether, benzo 18-crown-6 ether, and benzo 15-crown-5 ether) functionalized enamines derivatives from amino benzo crown ether (4-amino dibenzo 18-crown-6 ether, 4-amino benzo 18-crown-6 ether, 4-amino benzo 15-crown-5 ether) and substituted 3-(dimethylamino)-1-phenylprop-2-en-1-one compounds have been synthesized. All the synthesized compounds were characterized by infrared, 1H NMR, 13C NMR, distortionless enhancement polarization transfer, and mass and elemental analysis techniques. The cation recognition property for benzo crown ether enamine 8a was studied by absorption and fluorescence spectroscopy.

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