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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 46, 2016 - Issue 2
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Original Articles

Copper nitrate–catalyzed α-bromination of aryl ketones with hydrobromic acid

Jianqiang WangCollege of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, China
,
Xiaolei WangCollege of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, China
,
Zong-Qiang NiuCollege of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, China
,
Jian WangCollege of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, China
,
Man ZhangCollege of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, China
&
Jing-Hua LiCollege of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou, ChinaCorrespondence[email protected]
Pages 165-168 | Received 29 Aug 2015, Published online: 08 Feb 2016
 
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ABSTRACT

An efficient method for α-bromination of aryl ketones, using the combination of molecular oxygen and aqueous hydrobromic acid as a brominating agent in the presence of the copper nitrate, has been developed. This catalytic system, which uses cheap and readily available reactants, shows good atom economy with water as the only by-product.

GRAPHICAL ABSTRACT

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