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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 46, 2016 - Issue 8
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Original Articles

Practical synthesis of β-isothiocyanato ketones from chalcones

Anastasia A. FesenkoDepartment of Organic Chemistry, Moscow Technological University, Moscow, Russian Federation
,
Pavel A. SolovyevDepartment of Organic Chemistry, Moscow Technological University, Moscow, Russian Federation
&
Anatoly D. ShutalevDepartment of Organic Chemistry, Moscow Technological University, Moscow, Russian FederationCorrespondence[email protected]
Pages 678-684 | Received 24 Dec 2015, Published online: 04 May 2016
 
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ABSTRACT

Practical synthesis of 1,3-diaryl-substituted 3-isothiocyanatopropan-1-ones based on the reaction of chalcones with thiocyanic acid generated in situ by treatment of thiocyanate ammonium with dilute sulfuric acid has been developed.

GRAPHICAL ABSTRACT

Acknowledgments

This research was financially supported by the Ministry of Education and Science of the Russian Federation (project part of government order, 4.1849.2014/K) and Russian Foundation for Basic Research (Grant No. 15-03-07564).

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