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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 47, 2017 - Issue 1
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Original Articles

Convenient, metal-free ipso-nitration of arylboronic acids using nitric acid and trifluoroacetic acid

Guodong ShenSchool of Chemistry and Chemical Engineering, School of Pharmacy, Liaocheng University, Shandong, ChinaCorrespondence[email protected]
,
Lingyu ZhaoSchool of Chemistry and Chemical Engineering, School of Pharmacy, Liaocheng University, Shandong, China
,
Wanxing LiuDepartment of Chemistry, Liaocheng Chemical Institute of Industrial Science, Liaocheng, Shandong, China
,
Xianqiang HuangSchool of Chemistry and Chemical Engineering, School of Pharmacy, Liaocheng University, Shandong, China
,
Huina SongSchool of Chemistry and Chemical Engineering, School of Pharmacy, Liaocheng University, Shandong, China
&
Tongxin ZhangSchool of Chemistry and Chemical Engineering, School of Pharmacy, Liaocheng University, Shandong, China
Pages 10-14 | Received 21 Jun 2016, Published online: 02 Dec 2016
 
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ABSTRACT

A feasible protocol for the direct ipso-nitration of arylboronic acids using trifluoroacetic acid and nitric acid as nitration reagent has been developed. Various aromatic nitro compounds are produced in moderate to good yields under the metal-free conditions. The method is operationally simple and regioselective, and might have potential application in industry.

GRAPHICAL ABSTRACT

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