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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 47, 2017 - Issue 11
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Original Articles

Copper powder-catalyzed coupling and cyclization of 1-bromoallyl bromides with amidine hydrochlorides leading to pyrimidines

Ha Kyeong LeeDepartment of Applied Chemistry, Kyungpook National University, Daegu, South Korea
,
Ho-Sang SohnDepartment of Materials Science and Metallurgical Engineering, Kyungpook National University, Daegu, South Korea
&
Chan Sik ChoDepartment of Applied Chemistry, Kyungpook National University, Daegu, South KoreaCorrespondence[email protected]
Pages 1046-1051 | Received 23 Mar 2016, Published online: 20 Apr 2017
 
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ABSTRACT

1-Bromoallyl bromides are coupled and cyclized with amidine hydrochlorides in DMF at 130 °C in the presence of a catalytic amount of copper powder along with K3PO4 to give pyrimidines in moderate to good yields.

GRAPHICAL ABSTRACT

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