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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 48, 2018 - Issue 21
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Articles

NMP-mediated chlorination of aliphatic alcohols with aryl sulfonyl chloride for the synthesis of alkyl chlorides

Dagui ZhengKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaCorrespondence[email protected]
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,
Liu-Liang MaoKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaView further author information
,
Xian-Hong ZhuKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaView further author information
&
An-Xi ZhouKey Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao, PR ChinaORCID Iconhttp://orcid.org/0000-0002-2143-0988View further author information
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Pages 2793-2800 | Received 19 Mar 2018, Published online: 30 Oct 2018
 
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Abstract

NMP-mediated chlorination of aliphatic alcohols has been developed for the synthesis of alkyl chlorides. This facile, efficient and practical approach used simple and readily available aryl sulfonyl chlorides as the chlorination reagent for the construction of C–Cl bond in good to excellent yields with mild conditions and broad substrate scope.

GRAPHICAL ABSTRACT

Additional information

Funding

The research work was supported by the financial support from the Science and Technology Research Projects of the Jiangxi Provincial Education Department [Nos. GJJ161059, GJJ151062 and GJJ14716].

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