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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 49, 2019 - Issue 7
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Articles

Consecutive addition esterification and hydrolysis of cyclic olefins catalyzed by multi-SO3H functionalized multi heteropolyanion-based ionic hybrids undersolvent-free conditions

Guocai ZhengDepartment of Materials Engineering, Ocean College, Minjiang University, Fuzhou, People’s Republic of China; ;Green Dyeing and Finishing Engineering Research Centre, Fujian University, Fuzhou, People’s Republic of China;View further author information
&
Xinzhong LiDepartment of Materials Engineering, Ocean College, Minjiang University, Fuzhou, People’s Republic of China; ;Green Dyeing and Finishing Engineering Research Centre, Fujian University, Fuzhou, People’s Republic of China;;State Key Laboratory of Structural Chemistry, Fuzhou, People’s Republic of China;;Fujian Engineering Research Center of New Chinese Lacquer Material, Fuzhou, People's Republic of ChinaCorrespondence[email protected];[email protected]
View further author information
Pages 933-941 | Received 08 Mar 2018, Published online: 08 Mar 2019
 
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Abstract

An efficient protocol for the synthesis of cycloalkyl carboxylates and alcohols from cyclic olefins is described. The cyclic olefins were converted to corresponding target molecules under solvent-free conditions catalyzed by two novel multi-SO3H functionalized multi heteropolyanion-based ionic hybrids through one-pot consecutive addition esterification and hydrolysis reactions. This approach has several advantages, including high yield, simple workup and simple purification.

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Funding

The authors thank the Natural Science Foundation of Fujian Province [No. 2016J01690, 2017J01584], Research Project of Fujian Province Education Department [No.JAT160373, 170453, and JK2016035], Open Subject of State Key Laboratory of Structural Chemistry [20170030], and Research Project of Minjiang University [No.MYK18004, 16003, and 16004] for financial support.

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