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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 50, 2020 - Issue 7
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ARTICLES

A one-pot three-step multicomponent synthesis of functionalized allyl dithiocarbamates using Baylis–Hillman reaction

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Pages 966-972 | Received 30 Nov 2019, Published online: 19 Feb 2020
 

Abstract

A one-pot, pseudo five-component, highly diastereoselective, and mild procedure for the synthesis of functionalized allyl dithiocarbamates is developed. The Baylis–Hillman (BH) reaction of aromatic (heteroaromatic) aldehydes and activated alkenes using DABCO, followed by acetylation of BH adducts with acetic anhydride in the presence of a catalytic amount of DMAP, and nucleophilic substitution reaction by in situ prepared dithiocarbamates from amines and CS2 are three steps of this protocol.

Graphical Abstract

Acknowledgments

We thank the research council of Kharazmi University for supporting this work.

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