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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 50, 2020 - Issue 12
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SYNTHETIC COMMUNICATIONS REVIEWS

Efficient synthesis of 2-amino-3-methylenephthalimides by a palladium-catalyzed intramolecular aminocarbonylation

Guoshuai PanCollege of Chemistry and Materials Science, Fujian Normal University, Fuzhou, People’s Republic of China; View further author information
,
Yumeng YuanCollege of Chemistry and Materials Science, Fujian Normal University, Fuzhou, People’s Republic of China; View further author information
,
Lv SuCollege of Chemistry and Materials Science, Fujian Normal University, Fuzhou, People’s Republic of China; View further author information
,
Xiaofeng ZhangCollege of Chemistry and Materials Science, Fujian Normal University, Fuzhou, People’s Republic of China; Correspondence[email protected]
View further author information
&
Qiufeng HuangCollege of Chemistry and Materials Science, Fujian Normal University, Fuzhou, People’s Republic of China; ;Fujian Key Laboratory of Polymer Materials, Fuzhou, People’s Republic of ChinaCorrespondence[email protected]
ORCID Iconhttp://orcid.org/0000-0002-0166-2140View further author information
ORCID Icon
Pages 1892-1898 | Received 02 Feb 2020, Published online: 06 May 2020
 
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Abstract

An efficient synthesis of 2-amino-3-methylenephthalimide through palladium-catalyzed intramolecular aminocarbonylation has been developed. The reaction carried out under atmospheric pressure of CO and provided diversified 2-amino-3-methylenephthalimides in reasonable to good yields from o-iodoacetophenone phenylhydrazone, which are readily derived from phenylhydrazines and 2-iodoacetophenones.

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Funding

Financial support from NSFC [Grant Nos. 21872028], Natural Science Foundation of Fujian Province [Grant No. 2017J01572], the Foundation of Fujian Educational Committee [Grant No.JZ160424], and the Fujian Province University Fund for New Century Excellent Talents for Financial Support.

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