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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 50, 2020 - Issue 21
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Articles

Gram scale synthesis of alpha-cyanoalkylboronic esters via direct B–B and C–N bond cleavage

Sushree Ranjan SahooDepartment of Chemistry, National Institute of Technology, Rourkela, Odisha, IndiaView further author information
&
Debayan SarkarDepartment of Chemistry, National Institute of Technology, Rourkela, Odisha, IndiaCorrespondence[email protected]
View further author information
Pages 3308-3313 | Received 14 May 2020, Published online: 03 Aug 2020
 
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Abstract

A direct metal-free approach for the synthesis of alpha-cyanoalkylboronic esters from bis-diboron ester and azobis-nitrile compound is reported under ambient temperature and pressure via a free radical procedure.

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Funding

We sincerely acknowledge the Department of Science and Tech-nology (DST), Government of India [Grant No. EEQ/2016/000518], INSPIRE-DST, Government of India [Grant 04/2013/000751] and NIT Rourkela.

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