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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 51, 2021 - Issue 4
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Articles

Hantzsch-like synthesis of the 10b-azachrysenes, spirocyclic oxindole of 10b-azachrysene and 10a-azaphenanthrene utilizing 2-(6,7-dimethoxy-3,4-dihydroisoquinolin-1-yl)acetonitrile as a precursor

Mohamed A. Mohamed TelebDepartment of Chemistry, Faculty of Science, Cairo University, Giza, Egypt
,
Hamdi M. HassaneenDepartment of Chemistry, Faculty of Science, Cairo University, Giza, EgyptORCID Iconhttps://orcid.org/0000-0003-0963-4192
ORCID Icon,
Ismail A. AbdelhamidDepartment of Chemistry, Faculty of Science, Cairo University, Giza, EgyptCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0003-1220-8370
ORCID Icon &
Fatma M. SalehDepartment of Chemistry, Faculty of Science, Cairo University, Giza, EgyptORCID Iconhttps://orcid.org/0000-0003-0451-4802
ORCID Icon
Pages 553-562 | Received 28 Aug 2020, Published online: 02 Nov 2020
 
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Abstract

We report an efficient synthesis of 10b-azachrysenes and 10a-azaphenanthrene derivatives via the Hantzsch-like reaction of heterocyclic aldehydes and 2-(6,7-dimethoxy-3,4-dihydroisoquinolin-1-yl)acetonitrile with either dimedone or 3-aminocrotononitrile in acetic acid.

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