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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 53, 2023 - Issue 1
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Articles

3-Nitro-2(1H)-quinolone derivatives as 2π components in 1,3-dipolar cycloadditions of azomethine ylides: A new synthesis of pyrrolo[3,4-c]quinolines

Márk Molnára Servier Research Institute of Medicinal Chemistry, Budapest, Hungary
,
Tamás Johna Servier Research Institute of Medicinal Chemistry, Budapest, Hungary
,
András Dancsób EGIS Pharmaceuticals Ltd, Budapest, Hungary
&
Miklós Nyergesa Servier Research Institute of Medicinal Chemistry, Budapest, HungaryCorrespondence[email protected]
Pages 76-84 | Received 22 Sep 2022, Published online: 11 Dec 2022
 
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Abstract

The 1,3-dipolar cycloaddition of 3-nitro-2(1H)-quinolones with ester-stabilized azomethine ylides derived from sarcosine ester and various aromatic aldehydes has been investigated. The structure and stereochemistry of cycloadducts were studied in detail by X-ray and NMR spectroscopy methods.

GRAPHICAL ABSTRACT

Acknowledgments

The authors acknowledge Barbara Balázs and Tamás Gáti for spectral measurements.

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