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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 5
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Original Articles

New Method for the Synthesis of Benzyl Alkyl Ethers Mediated by FeSO4

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Pages 720-728 | Received 17 Sep 2009, Published online: 31 Jan 2011
 

Abstract

The synthesis of benzyl alkyl ethers from benzyl bromides and alcohols using FeSO4 as a recoverable and reusable mediator has been described without use of base and cosolvent under mild conditions.

ACKNOWLEDGMENT

The authors gratefully acknowledge the Department of Science and Technology, New Delhi, India, for the financial support of this project under the Green Chemistry Task Force Scheme (No. SR/S5/GC-02A/2006).

Notes

Note. Conditions: 1a (3.0 mmol), 2 (5.0 mL), reflux, 12 h.

a GC yields based on starting benzyl bromide; numbers in parantheses are isolated yields.

b Temperature at 110 °C.

a Isolated yields under the optimized conditions of Table 1.

b GC yields.

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