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Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 13, 1983 - Issue 4

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Reagents and Synthetic Methods 25. A New Method for the Synthesis of Acyl Azides from Carboxylic Acids and Sodium Azide Induced by Phenyl Dichlorophosphate

J. M. Lago Dpto. de Quïmica Orgánica, Facultad de Ciencias, Químicas San, Sebastián, Spain

A. Arrieta Dpto. de Quïmica Orgánica, Facultad de Ciencias, Químicas San, Sebastián, Spain

C. Palomo Dpto. de Quïmica Orgánica, Facultad de Ciencias, Químicas San, Sebastián, Spain

Pages 289-296 | Published online: 05 Dec 2006

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https://doi.org/10.1080/00397918308066978

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Abstract

Carbonyl azides are obtained in high yields by a one-pot method from carboxylic acids and sodium azide by means of phenyl dichlorophosphate reagent.

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