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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 14, 1984 - Issue 12
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Original Articles

A Novel and Cheap Synthesis of Artemisia Ketone1 (3,3,6-Trimethylhepta-L,5-Dien-4-One)

Lucien Stella L.A. 109 C.N.R.S., Laboratoire de Chimie Organique B, Université d'Aix-Marseille III, Rue H. Poincaré, 13397, Marseille Cedex 13, France
&
Ali Amrollah-madjdabadi L.A. 109 C.N.R.S., Laboratoire de Chimie Organique B, Université d'Aix-Marseille III, Rue H. Poincaré, 13397, Marseille Cedex 13, France; Institut de Chimie des Substances Naturelles, C.N.R.S., 91190, Gif sur Yvette, France
Pages 1141-1147 | Published online: 06 Dec 2006
 
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Abstract

The Sequential dialkylation of dimethylaminoacetonitrile with first methallylchloride and then prenylbromide is performed at room temperature using K2CO3 in DMF. Subsequent hudrolysis and isomerisation offord artemisia ketone in 77% overall yield.

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