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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 2
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Original Articles

A Novel Synthesis of Steroidal Δ4,3,6-Diones Using Pyridinium Chlorochromate (PCC)

Edward J. Parish Department of Chemistry Auburn University, AL 36849-5312
,
Stephen A. Kizito Department of Chemistry Auburn University, AL 36849-5312
&
Robert W. Heidepriem Department of Chemistry Auburn University, AL 36849-5312
Pages 223-230 | Received 03 Aug 1992, Published online: 23 Sep 2006
 
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Abstract

Pyridinium chlorochromate (PCC), in refluxing benzene, has been found to be an effective and convenient reagent for the oxidation of steroidal Δ5-3β-tetrahydropyranyl ethers to the corresponding Δ4-3,6-diones in high yield.

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