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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 10
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Original Articles

Samarium Diiodide-Induced Reduction of Elemental Selenium Leading to a Selenolate Anion Species. A Selective Synthesis of Diacyl Diselenides

Xueshun Jia Department of Chemistry, Hangzhou University, Hangzhou, 310028 P.R., China
,
Yongmin Zhang Department of Chemistry, Hangzhou University, Hangzhou, 310028 P.R., China
&
Xunjun Zhou Department of Chemistry, Hangzhou University, Hangzhou, 310028 P.R., China
Pages 1403-1408 | Received 01 Dec 1992, Published online: 23 Sep 2006
 
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Abstract

Elemental selenium was reduced by samarium diiodide in THF to produce selenolate anion species which reacted with acyl chlorides to give diacyl diselenides in good yields under mild and neutral conditions.

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