Preparation of Diallyl Ketals

John B. Brogan Department of Chemistry, University of New Hampshire Durham, New Hampshire, 03824

Judson E. Richard Department of Chemistry, University of New Hampshire Durham, New Hampshire, 03824

Charles K. Zercher Department of Chemistry, University of New Hampshire Durham, New Hampshire, 03824

Abstract

A general method for the preparation of diallyl acetals and ketals is reported. The reaction is performed well below room temperature, thereby eliminating any competing Claisen rearrangement. These mild reaction conditions also facilitate ketal formation on methyl levulinate 1 with no transesterification.

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Preparation of Diallyl Ketals

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Preparation of Diallyl Ketals

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