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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 8
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Original Articles

Mild and Fast Deoxygenation of Aromatic Carbonyl Compounds by Dimethylamine Borane / Titanium Tetrachloride

Eckehard V. Dehmlow Fakultät für Chemie, Universität Bielefeld Postfach, 100131, D-33501, Bielefeld, Germany
,
Thomas Niemann Fakultät für Chemie, Universität Bielefeld Postfach, 100131, D-33501, Bielefeld, Germany
&
Anke Kraft Fakultät für Chemie, Universität Bielefeld Postfach, 100131, D-33501, Bielefeld, Germany
Pages 1467-1472 | Received 27 Sep 1995, Published online: 15 Aug 2006
 
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Abstract

The title reaction proceeds in dichloromethane at room temperature within ½ hour. Benzylic alcohols are intermediates. TiCl4 can be replaced by other (although less effective) Lewis acids such as AlCl3, BF3·ether, FeCl3.

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