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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 17
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Original Articles

Surface-Mediated Solid Phase Reaction. IX. A Convenient Procedure for Aldol Reaction of Ketene Silyl Acetals with Aldehydes on the Solid Surface of Alumina

Brindaban C. Ranu Department of Organic Chemistry, Indian Association for the Cultivation of Science Jadavpur, Calcutta, 700032, India
,
Manika Saha Department of Organic Chemistry, Indian Association for the Cultivation of Science Jadavpur, Calcutta, 700032, India
&
Sanjay Bhar Department of Organic Chemistry, Indian Association for the Cultivation of Science Jadavpur, Calcutta, 700032, India
Pages 3065-3077 | Received 16 Dec 1996, Published online: 22 Aug 2006
 
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Abstract

The aldol reaction of ketene silyl acetals with aldehydes proceeds efficiently on the solid surface of alumina impregnated with anhydrous zinc chloride under sonication providing aldol products in high yields and with good stereoselectivity.

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