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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 19
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Original Articles

Dinitrogen Tetroxide Complexes of Iron and Copper Nitrates as New Reagents for Selective Mono- and Dinitration of Phenolic Compounds

H. Firouzabadi Department of Chemistry, Shiraz University, Shiraz, 71454, Iran
,
N. Iranpoor Department of Chemistry, Shiraz University, Shiraz, 71454, Iran
&
M. A. Zolfigol Department of Chemistry, Shiraz University, Shiraz, 71454, Iran
Pages 3301-3311 | Received 11 Jan 1997, Published online: 22 Aug 2006
 
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Abstract

Fe(NO3)3. 1.5 N2O4 and Cu(NO3)2. N2O4 are easily prepared reagents for the efficient and selective mono- or dinitration of phenolic compounds. In comparison with metal nitrates, these complexes resemble a synergetic effect on the rates and the yields of the reactions. High ratio of p-nitrophenol formation vs o-nitrophenol is also observed in the mononitration reactions.

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