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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 12
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Original Articles

Practical Phase-Transfer Synthesis of N-(Ethoxycarbonyl)Phthalimide and Its Analogues

Renata Siedlecka Institute of Organic Chemistry, Biochemistry and Biotechnology Technical University, 50-370, Wrocław, Poland
&
Jacek Skarzewski Institute of Organic Chemistry, Biochemistry and Biotechnology Technical University, 50-370, Wrocław, Poland
Pages 2081-2086 | Received 23 Jan 1997, Published online: 22 Aug 2006
 
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Abstract

Potassium imides are N-acylated with ethyl chloroformate in the presence of tetrabutylammonium chloride to form the corresponding N-etyhoxycarbonyl derivatives, useful agents for N-protection of primary amines.

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