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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 5
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Original Articles

A convenient One-Pot Synthesis of an Unsymmetrical Propane-1,3-diamine BRL 61010A

Robin P Attrill Synthetic Chemistry SmithKline Beecham Pharmaceuticals, New Frontiers Science Park, Third Avenue, Harlow, Essex, CM19 5AW
,
Thomas W Ramsay Synthetic Chemistry SmithKline Beecham Pharmaceuticals, New Frontiers Science Park, Third Avenue, Harlow, Essex, CM19 5AW
,
Graham R Slater Synthetic Chemistry SmithKline Beecham Pharmaceuticals, New Frontiers Science Park, Third Avenue, Harlow, Essex, CM19 5AW
&
Paul Smith Synthetic Chemistry SmithKline Beecham Pharmaceuticals, New Frontiers Science Park, Third Avenue, Harlow, Essex, CM19 5AW
Pages 827-833 | Received 06 Sep 1998, Published online: 17 Sep 2007
 
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Abstract

The one-pot condensation of N-methylhomoveratrylamine with acrolein followed by in situ reductive amination with 3,4-dimethoxyaniline to give an unsymmetrical propane 1,3-diamine in excellent yield is described.

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