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Journal of Coordination Chemistry Volume 61, 2008 - Issue 4
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Original Articles

Syntheses, structure and magnetism of a new linear-chain coordination polymer [[Co(TMA)2(4,4′-bipyridine)2] · H2O]n [TMA=Trimesate]

Huan-Ran Xing College of Chemistry and Materials Engineering, Wenzhou University, Wenzhou, Zhejiang 325027, P. R. China
,
Xin-Hua Li College of Chemistry and Materials Engineering, Wenzhou University, Wenzhou, Zhejiang 325027, P. R. ChinaCorrespondence[email protected]
&
Qian Shi College of Chemistry and Materials Engineering, Wenzhou University, Wenzhou, Zhejiang 325027, P. R. China
Pages 499-507 | Received 03 Feb 2007, Accepted 24 Mar 2007, Published online: 22 Feb 2008
 
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Abstract

A linear-chain one-dimension polymeric complex of Co(II), [[Co(TMA)2(4,4′-bipyridine)2] · H2O] n has been synthesized and characterized. The complex crystallizes in the monoclinic system, space group P2(1)/c with a = 11.344(3) Å, b = 15.880(4) Å, c = 23.436(5) Å, β = 117.831(10)°, V = 3733.5(16) Å3 and D c = 1.437 g cm−3. The effective magnetic moment for this complex indicates that there is almost no ferromagnetic coupling between the Co(II) ions and the magnetic behavior is due to the isolated Co(II).

Acknowledgements

This work was supported by the Zhejiang Provincial Natural Science Foundation of China (grant No. Y404294), “151” distinguished person foundation of Zhejiang Province and the Nation Natural Science Foundation of China (grant No. 20601021).

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