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Journal of Coordination Chemistry Volume 61, 2008 - Issue 5
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Original Articles

Syntheses and structures of three manganese coordination polymers with 1,4-bis(imidazol-1-yl)butane

Yu-Mei Zhang Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123, P.R. China
,
Yuan Yang Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123, P.R. China
,
Hai-Yan Ge Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123, P.R. China
,
Bao-Long Li Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123, P.R. ChinaCorrespondence[email protected]
&
Yong Zhang Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215123, P.R. China
Pages 750-759 | Received 12 Feb 2007, Accepted 05 Apr 2007, Published online: 03 Mar 2008
 
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Abstract

Three manganese coordination polymers [Mn(bimb)2(NCS)2] n (1), [Mn(bimb)2(dca)2] n (2) and [Mn(bimb)2(N3)2] n (3) (bimb = 1,4-bis(imidazol-1-yl)butane, dca = dicyanamide) were synthesized and characterized by X-ray crystallography, IR and thermogravimetric analysis. In 1 and 2, each Mn(II) links two Mn(II) atoms by double bimb ligands and extends to form a one-dimensional double chain structure containing the Mn2(bimb)2 22-member metallocycle. 3 constructs a two-dimensional (4,4) network linked by bimb bridges.

Acknowledgement

This work was supported by the Natural Science Foundation of the Jiangsu Province (No. BK2006049), the Funds of Key Laboratory of Organic Synthesis of Jiangsu Province (No. JSK0612).

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