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Journal of Coordination Chemistry Volume 65, 2012 - Issue 8
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Original Articles

Synthesis, structural characterization, and properties of an entangled metal–organic framework based on a flexible dicarboxylate and a rigid N-donor

Jian-Qiang Liu Guangdong Medical College, School of Pharmacy, Dongguan 523808, P.R. ChinaCorrespondence[email protected]
,
Jian Wu College of Chemistry and Chemical Engineering, Guangxi University for Nationalities, Nanning, Guangxi 530006, P.R. China
,
Yao-Yu Wang Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of the Ministry of Education, Shaanxi Key Laboratory of Physico-Inorganic Chemistry, Department of Chemistry, Northwest University, Xi’an 710069, P.R. China
&
De-Yun Ma College of Chemistry and Chemical Engineering, Zhaoqing University, Zhaoqing 526021, P.R. China
Pages 1303-1310 | Received 18 Nov 2011, Accepted 23 Jan 2012, Published online: 26 Mar 2012
 
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Abstract

Self-assembly of manganese acetate with 1,3-bis(4-carboxy-phenoxy)propane (H2bcp) and 1,2-bis(4-pyridyl)ethene (bpe) under solvothermal conditions yielded a polymer {[Mn2(bcp)2(bpe)(DMF)]} n (1), which shows 2-D → 3-D inclined interpenetration with polyrotaxane character. The magnetic behavior of 1 shows antiferromagnetic exchange between Mn magnetic centers.

Acknowledgments

We gratefully acknowledge financial support of this work by Guangdong Medical College with Doctor start-up Foundation (B2010009), and greater contribution from Dr B. Liu.

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