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Journal of Coordination Chemistry Volume 66, 2013 - Issue 3
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Articles

Three inorganic–organic hybrid compounds based on Keggin polyoxometalate and transition metal complexes: crystal structures and electrochemical properties

XIAOYU LIU Key Laboratory of Cluster Science of Ministry of Education, Department of Chemistry, Beijing Institute of Technology, Beijing, PR China; Beijing Union University, Beijing, PR China
,
HAILIANG NIE Key Laboratory of Cluster Science of Ministry of Education, Department of Chemistry, Beijing Institute of Technology, Beijing, PR China
,
LI WANG Key Laboratory of Cluster Science of Ministry of Education, Department of Chemistry, Beijing Institute of Technology, Beijing, PR China
&
RUDAN HUANG Key Laboratory of Cluster Science of Ministry of Education, Department of Chemistry, Beijing Institute of Technology, Beijing, PR ChinaCorrespondence[email protected]
Pages 444-452 | Received 27 Jul 2012, Accepted 19 Oct 2012, Published online: 29 Jan 2013
 
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Abstract

Polyoxometalate (POM)-based coordination polymers, [Cu(L)2][SiW12O40]·4py·H2O (1), [Ag(py)2]4[SiW12O40] (2) and [Co(L)3]2[SiW12O40]·py·7H2O (3) (L = pyridine-2-carboxylic acid, py = pyridine), have been obtained hydrothermally and characterized by elemental analyses, IR and single-crystal X-ray diffraction analyses. Electrochemical properties are also investigated.

Acknowledgements

This work was financially supported by the National Natural Science Foundation of China (No. 20971014, No. 20771013), the 111 Project (B07012) in China, the Beijing Natural Science Foundation (No. 2112037), and the Foundation for basic research by Beijing Institute of Technology (No. 20091742012).

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