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Journal of Coordination Chemistry Volume 66, 2013 - Issue 21
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Original Articles

Two new zinc(II) metal-organic frameworks based on 1,4-bis(2-methyl-imidazol-1-yl)butane: synthesis, structures, and properties

Jun-Cheng JinAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. ChinaCorrespondence[email protected]
,
Wen-Quan TongAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. China
,
Cheng-Gen XieAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. China
,
Wen-Gui ChangAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. China
,
Guang-Nian XuAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. China
,
Ju WuAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. China
,
Lin-Gang LiAnhui Provincial Laboratory of Biomimetic Sensor and Detecting Technology, Engineering Research Center for Development and Application of Solar Photovoltaic Materials, West Anhui University, Lu’an, P.R. China
,
Zheng-Quan YanKey Laboratory of Synthetic and Natural Functional Molecule Chemistry of Ministry of Education, Department of Chemistry, Northwest University, Xi’an, P.R. China
&
Yao-Yu WangKey Laboratory of Synthetic and Natural Functional Molecule Chemistry of Ministry of Education, Department of Chemistry, Northwest University, Xi’an, P.R. China
 show all
Pages 3697-3705 | Received 03 Jul 2013, Accepted 04 Sep 2013, Published online: 15 Nov 2013
 
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Abstract

Two new zinc(II) metal-organic compounds, {[Zn(ADC)(bib)]·CH3OH·H2O}n (1) and [Zn(ADA)(bib)]n (2) (H2ADC = 1,3-adamantanedicarboxylic acid, H2ADA = 1,3-adamantanediacetic acid, bib = 1,4-bis(2-methyl-imidazol-1-yl)butane), have been synthesized and characterized. In 1, zinc(II) ions are bridged by ADC to form a 1-D chain. The chains are further connected by bib to form a 2-D wave structure. In 2, zinc(II) ions are bridged by two ADA to form a 1-D looped chain, and then the 1-D looped chain is connected through bib resulting in a 2-D network. Fluorescent properties, TG analysis, and XRPD for 1 and 2 are also measured and discussed.

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