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Journal of Coordination Chemistry Volume 73, 2020 - Issue 8
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Articles

Coordination modes of salicylaldehyde derivatives in the ruthenium(II) nitrosyl and bis(2,2′-bipyridine) ruthenium(II) complexes

Chong ChenInstitute of Molecular Engineering and Applied Chemistry, Anhui University of Technology, Ma’anshan, Anhui, P. R. ChinaView further author information
,
Jiao JiInstitute of Molecular Engineering and Applied Chemistry, Anhui University of Technology, Ma’anshan, Anhui, P. R. ChinaView further author information
,
Chang-Jiu WangInstitute of Molecular Engineering and Applied Chemistry, Anhui University of Technology, Ma’anshan, Anhui, P. R. ChinaView further author information
,
Ai-Quan JiaInstitute of Molecular Engineering and Applied Chemistry, Anhui University of Technology, Ma’anshan, Anhui, P. R. ChinaView further author information
&
Qian-Feng ZhangInstitute of Molecular Engineering and Applied Chemistry, Anhui University of Technology, Ma’anshan, Anhui, P. R. ChinaCorrespondence[email protected] [email protected]
View further author information
Pages 1306-1313 | Received 24 Dec 2019, Accepted 01 May 2020, Published online: 20 May 2020
 
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Abstract

Treatment of [Ru(NO)Cl3(PPh3)2] with one equivalent of 3,5-dibromosalicylaldehyde in the presence of triethylamine gave the ruthenium(II) nitrosyl complex [Ru(NO)(κ2-C,O-salBr2)Cl(PPh3)2] (1). Interaction of [Ru(bpy)2Cl2]·2H2O with one equivalent of 5-chlorosalicylaldehyde in ethanol/N,N′-dimethylformamide afforded the bis(2,2′-bipyridine)ruthenium(II) complex [Ru(bpy)2(κ2-O,O-salCl)](PF6) (2). Complexes 1 and 2 were well characterized by infrared, proton nuclear magnetic resonance spectroscopies along with microanalyses and their molecular structures were determined by single-crystal X-ray diffraction.

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Disclosure statement

No potential conflict of interest was reported by the authors.

Additional information

Funding

This project was supported by the Natural Science Foundations of China (21372007).

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