) and 4-n-Pentylphenyl 4-n-Decyloxybenzthiolate (
)The title compounds have been prepared and their phase behaviour studied. They have earlier been reported to show a new type of smectic phase (smectic Y). However, X-ray diffraction measurements show this to be a smectic J phase. The measured tilt angle is 20° for 
and 16° for 
.
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