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Phase Transitions
A Multinational Journal
Volume 81, 2008 - Issue 11-12
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Original Articles

Synthesis, microstructure and dielectric properties of (1−x)PSN−xPLuN

B. Garbarz-Glos Institute of Physics, Pedagogical University, Krakow, PolandCorrespondence[email protected]
,
W. Śmiga Institute of Physics, Pedagogical University, Krakow, Poland
,
M. Dambekalne Institute of Solid State Physics, University of Latvia, Riga, Latvia
,
A. Kalvane Institute of Solid State Physics, University of Latvia, Riga, Latvia
,
M. Antonova Institute of Solid State Physics, University of Latvia, Riga, Latvia
,
R. Bujakiewicz-Korońska Institute of Physics, Pedagogical University, Krakow, Poland
,
I. Jankowska-Sumara Institute of Physics, Pedagogical University, Krakow, Poland
,
D. Sitko Institute of Physics, Pedagogical University, Krakow, Poland
,
J. Suchanicz Institute of Physics, Pedagogical University, Krakow, Poland
,
A. Sternberg Institute of Solid State Physics, University of Latvia, Riga, Latvia
&
M. Burzyńska Institute of Physics, Pedagogical University, Krakow, Poland
 show all
Pages 1065-1071 | Received 18 May 2008, Accepted 11 Jun 2008, Published online: 04 Dec 2010
 
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Abstract

Ceramic lead niobates and their solid solutions PSN–PLuN (pure lutecium niobate) were synthesized by solid state reactions. The sequence of phases formed at PSN–PLuN synthesis has been studied by X-ray analysis. Their symmetry changed from rhombohedral for PSN to pseudo-monoclinic for the 0.75PSN–0.25PLuN compositions. The performed EDS investigations revealed that the samples PSN–PLuN are perfectly sintered. They contain a little glassy phase and their grains are well shaped. The increase of lutecium content in the examined solid solution caused downward shift of the temperature of the phase transition. The decrease of the achieved permittivity values ϵ was observed as well.

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