This article investigates the influence factors of reagent ratio, pH, stirring intensity, sintering temperature along with ultrasonic wave to particle size, distribution of nanoziconium dioxide in recombination surfactant system. The optimized reagent ratio (wt) of cyclohexan, OP‐10, n‐Amyl alcohol, zircon salt solution are 55%, 17.5%, 17.5%, 10%, respectively. At pH=8.7, the size of nanozirconium oxide has the priority of smaller (<10 nm), narrower particle size distribution and better performance in W/O form.
Acknowledgments
This research is supported in part by Natural Science Foundation of China and Mid‐young Scientists in Shandong Province, and by the Visiting Scholar Foundation of Key Lab in the University.