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International Journal of Environmental Analytical Chemistry Volume 47, 1992 - Issue 3
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Original Articles

Determination of Alkylphenol Ethoxylates and Their Acetic Acid Derivatives in Drinking Water by Particle Beam Liquid Chromatography/Mass Spectrometry

Linda B. Clark Dept. Food Science, Cook College, Rutgers University, New Brunswick, NJ, 08903, USA
,
Robert T. Rosen Center for Advanced Food Technology, Cook College, Rutgers University, New Brunswick, NJ, 08903, USA
,
Thomas G. Hartman Center for Advanced Food Technology, Cook College, Rutgers University, New Brunswick, NJ, 08903, USA
,
Judith B. Louis Div. Science and Research, Dept. Environmental Protection and Energy, CN 409, Trenton, NJ, 08625, USA
,
I. H. Suffet Department of Chemistry, Environmental Studies Institute, Drexel University, Philadelphia, PA, 19104, USA
,
R. L. Lippincott Department of Chemistry, Environmental Studies Institute, Drexel University, Philadelphia, PA, 19104, USA
&
Joseph D. Rosen Dept. Food Science, Cook College, Rutgers University, New Brunswick, NJ, 08903, USA
 show all
Pages 167-180 | Received 15 Jul 1991, Published online: 24 Sep 2006
 
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Abstract

Particle beam liquid chromatography/mass spectrometry (PB/LC/MS) was used to analyze finished drinking water for non-volatile organic compounds. 500 liters of finished water were extracted with an on-line continuous liquid/liquid extractor with dichloromethane at pH 7.4. PB/LC/MS was an excellent tool to detect and identify ng/L concentrations of alkylphenol polyethoxylates (n = 3−8), materials which went undetected by on-column gas chromatography/mass spectrometry. In addition, alkylphenol polyethoxylate carboxylates with 2–7 degrees of ethoxylation could be detected without chemical derivatization.

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