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Polymer-Plastics Technology and Engineering Volume 53, 2014 - Issue 6
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Original Articles

Preparation and Characterization of Acrylate Copolymers Modified by Fluorine and Silicon for Application in Release Films

Shuna Yu School of Chemistry and Chemical Engineering, Southeast University Jiangsu Optoelectronic Functional Materials and Engineering Laboratory, Nanjing, P.R. China
,
Yuming Zhou School of Chemistry and Chemical Engineering, Southeast University Jiangsu Optoelectronic Functional Materials and Engineering Laboratory, Nanjing, P.R. ChinaCorrespondence[email protected].
,
Tao Zhang School of Chemistry and Chemical Engineering, Southeast University Jiangsu Optoelectronic Functional Materials and Engineering Laboratory, Nanjing, P.R. China
&
Man He School of Chemistry and Chemical Engineering, Southeast University Jiangsu Optoelectronic Functional Materials and Engineering Laboratory, Nanjing, P.R. China
Pages 531-538 | Published online: 16 Apr 2014
 
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Abstract

Fluorine-silicone acrylate copolymers were synthesized with vinyltriethoxysilane (VTES), methyl hexafluorobutyl acrylate (HFMA), and other acrylate monomers by free radical polymerization. Further studies were directed at the water absorption ratio, contact angle and anti-adhesive performance of the films. The results indicated that the copolymers had narrow molecular weight distribution and high temperature stability. The films coated by copolymers showed excellent water/oil repellency with the contact angles of water and diiodomethane of 108.2° and 78.0°, respectively. Anti-adhesive performance testing demonstrated that the films had low peel strength, high residual adhesion rate and excellent water and solvent resistance.

Notes

R: The FSA copolymer chain.

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