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Nucleosides and Nucleotides Volume 18, 1999 - Issue 6-7
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OLIGONUCLEOTIDES I. PROGRESS IN THE SYNTHESIS, BUILDING BLOCKS, AND HYDROLYTIC PROPERTIES

An Improved Method for the Preparation of 4-Cyano-2-butenyl-deoxyribonucleosidephosphoramidites

G. Duckworth Cruachem Ltd Todd Campus, West of Scotland Science Park, Acre Road, Glasgow, Scotland, G20 OUA
&
J. Ackroyd Cruachem Ltd Todd Campus, West of Scotland Science Park, Acre Road, Glasgow, Scotland, G20 OUA
Pages 1227-1229 | Published online: 04 Oct 2006
 
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Abstract

An improved alternative synthesis of 4-cyano-2-butenyldeoxy nucleosidephosphoramidites in > 100g quantities is described via reaction of the phosphordiamidites with 4-cyano-2-buten-1-ol.

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