Abstract
We describe a technique for making electrical transport measurements in a diamond anvil cell at liquid helium temperature having in situ pressure measurement option, permitting accurate pressure determination at any low temperature during the resistance measurement scan. In general, for four-probe resistivity measurements on a polycrystalline sample, four fine gold wires are kept in contact with the sample with the help of the compression from the soft solid (usually alkali halides such as NaCl, KCl, etc.) acting as a pressure-transmitting medium. The actual pressure on the sample is underestimated if not measured from a ruby sphere placed adjacent to the sample and at that very low temperature. Here, we demonstrate the technique with a quasi-four-probe resistance measurement on an Fe-based superconductor in the temperature range 1.2–300 K and pressures up to 8 GPa to find an improved pressure dependence of the superconducting transition temperature.
Acknowledgements
The author is thankful to Pallavi S. Malavi for her help at various stages of the development of the facility and during the measurements. He is also thankful to Surinder M. Sharma and Karl Syassen for their support and suggestions during the development of the facility and insightful discussions during the investigation and analysis of the data.