Ultrafine grain development in copper during multidirectional forging at 195 K

Abstract

Strain-induced evolution of ultrafine grains in pure copper was studied in multidirectional forging (MDF) at 195 K. The stress–strain behaviour was characterized by rapid strain hardening during early processing and the rate of strain hardening gradually decreased with straining, leading to an apparent steady-state flow at large cumulative strains of more than 5. The structural changes were associated with the development of high-density microshear bands crossed by MDF. The new fine grains 0.16 µm in size, which was smaller than the subgrain size evolved during early deformation, were evolved primarily at microshear band intersections, and then the new fine grains filled out the whole sample as the number of microshear band intersections increased at large strains. This is essentially similar to continuous dynamic recrystallization. The size of new grains can be expressed by a power law function of flow stress with a grain size exponent of about –0.3. The kinetics of the strain-induced grain evolution is analyzed and the mechanisms are discussed.

Acknowledgments

The authors acknowledge with gratitude the financial support received from the Ministry of Education, Science and Culture, Japan, and the Japan Research Institute Advanced Copper-Base Materials and Technologies under grants of scientific research. One of the authors (A.B.) would like to express his thanks to the Tokyo Institute of Technology for providing a scientific fellowship.