Texture and grain boundary character distribution (GBCD) in rapidly solidified and annealed Fe–6·5 mass% Si ribbons

Abstract

The type and frequency of grain boundaries, the so-called grain boundary character distribution (GBCD), has been determined in rapidly solidified and subsequently annealed Fe-6·5 mass% Si alloy ribbon by the scanning electron microscopy-electron channelling pattern (SEM-ECP) technique. High frequencies of low-angle boundaries and coincidence boundaries with Σ3, Σ9, Σ11, Σ17 and Σ19 were observed in a fully annealed ribbon with well defined {110} texture. The total frequency of low-angle boundaries and coincidence boundaries is almost one-half of all grain boundaries. The coincidence boundaries which occurred more frequently are exactly those predicted theoretically from the coincidence orientations for 〈110〉 rotation in cubic crystals, similar to those observed previously in {100} textured ribbons of the same alloy produced by the same processing method. The presence of a close relationship between the type of texture and GBCD has been confirmed by experiment on differently textured ribbons of the same material.