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International Journal of Polymer Analysis and Characterization Volume 20, 2015 - Issue 3
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Original Articles

Solution Behavior of Hyperbranched Polymethylsilsesquioxane with Intramolecular Cycles

Alina I. AmirovaInstitute of Macromolecular Compounds, Russian Academy of Sciences, St. Petersburg, RussiaCorrespondence[email protected]
,
Olga V. GolubInstitute of Macromolecular Compounds, Russian Academy of Sciences, St. Petersburg, Russia
,
Ivan B. MeshkovN.S. Enikolopov Institute of Synthetic Polymer Materials, Russian Academy of Sciences, Moscow, Russia
,
Dmitry A. MigulinN.S. Enikolopov Institute of Synthetic Polymer Materials, Russian Academy of Sciences, Moscow, Russia
,
Aziz M. MuzafarovN.S. Enikolopov Institute of Synthetic Polymer Materials, Russian Academy of Sciences, Moscow, Russia
&
Alexander P. FilippovInstitute of Macromolecular Compounds, Russian Academy of Sciences, St. Petersburg, Russia
Pages 268-276 | Received 24 Nov 2014, Accepted 21 Jan 2015, Published online: 02 Apr 2015
 
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Abstract

Samples of hyperbranched polymethylsilsesquioxanes were synthesized at various polycondensation times and intramolecular cycle amounts. The samples were studied in solutions in toluene and hexane. It is shown that increasing the polycondensation duration results in the growth of number of cycles and intramolecular density that correlates with changes of molecular, hydrodynamic, and optic properties.

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