Abstract
Three new cassane-diterpene-lactones, methyl 1α,7β-diacetoxy-5α,12α-dihydroxy-cass-13(15)-en-16,12-olide-17β-carboxylate (1), methyl 7β-acetoxy-1α,5α,12α-trihydroxy-cass-13(15)-en-16,12-olide-17β-carboxylate (2), and 12α-ethoxyl-1α,6α,7β-triacetoxy-5α,14β-dihydroxy-cass-13(15)-en-16,12-olide (3), were isolated from the seeds of Caesalpinia minax Hance. Their structures were established on the basis of HR-ESI-MS, 1D and 2D NMR spectral analysis.
Acknowledgements
We thank Mrs Wen Li, Mr Yi Sha and Mr Weiming Cheng of the Analytical Centers of the Shenyang Pharmaceutical University for recording NMR spectra and HR-ESI-MS. This work was supported by the Natural Science Foundation Project of Heilongjiang Province (No. D200947).