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Journal of Asian Natural Products Research Volume 12, 2010 - Issue 11
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Original Articles

Concise total synthesis of largazole

Qiong Xiao Peking Union Medical College & Chinese Academy of Medical Sciences, Institute of Materia Medica, Beijing, 100050, China
,
Li-Ping Wang Peking Union Medical College & Chinese Academy of Medical Sciences, Institute of Materia Medica, Beijing, 100050, China
,
Xiao-Zhen Jiao Peking Union Medical College & Chinese Academy of Medical Sciences, Institute of Materia Medica, Beijing, 100050, China
,
Xiao-Yu Liu Peking Union Medical College & Chinese Academy of Medical Sciences, Institute of Materia Medica, Beijing, 100050, China
,
Qian Wu Peking Union Medical College & Chinese Academy of Medical Sciences, Institute of Materia Medica, Beijing, 100050, China
&
Ping Xie Peking Union Medical College & Chinese Academy of Medical Sciences, Institute of Materia Medica, Beijing, 100050, ChinaCorrespondence[email protected]
Pages 940-949 | Received 05 May 2010, Accepted 19 Jul 2010, Published online: 08 Nov 2010
 
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Abstract

The concise total synthesis of largazole was accomplished. The key step included the use of the Nagao thiazolidinethione auxiliary for the diastereoselective acetate aldol reaction and it acts as an acylating agent for the peptide formation.

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