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Journal of Asian Natural Products Research Volume 19, 2017 - Issue 6
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Original Articles

The synthesis of dendroflorin

Yi DengDepartment of Natural Medicinal Chemistry, Shanghai Insitute of Materia Medica, Chinese Academy of Sciences, Shanghai201203, China;University of Chinese Academy of Sciences, Beijing100049, China
,
Kun JiangDepartment of Natural Medicinal Chemistry, Shanghai Insitute of Materia Medica, Chinese Academy of Sciences, Shanghai201203, China
,
Mao-Jun CaiBiorun Pharm (Nantong) Co., Ltd., Nantong226413, China
,
Shi-Jin QuDepartment of Natural Medicinal Chemistry, Shanghai Insitute of Materia Medica, Chinese Academy of Sciences, Shanghai201203, China
,
Yi-Ru DaiCollege of Chemistry and Chemical Engineering, Shanghai University of Engineering Science, Shanghai201620, China
&
Chang-Heng TanDepartment of Natural Medicinal Chemistry, Shanghai Insitute of Materia Medica, Chinese Academy of Sciences, Shanghai201203, ChinaCorrespondence[email protected]
Pages 602-609 | Received 02 Mar 2017, Accepted 26 Apr 2017, Published online: 09 May 2017
 
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Abstract

The first synthesis of dendroflorin has been achieved in 10 steps with an overall yield of 5.5%. The key step in the synthesis features the biphenyl structure is built through Suzuki–Miyaura reaction. In addition, the ortho-localization effect induced by aromatic substituent during the bromination of intermediate 8 is also observed and discussed.

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