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Journal of Asian Natural Products Research Volume 8, 2006 - Issue 8
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Original Articles

Synthesis of three natural diosgenyl glycosides

S.-J. Hou Key Laboratory of Bioactive Substance and Resources Utilisation of Chinese Herbal Medicine (Peking Union Medical College), Ministry of Education, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Sciences, Beijing, 100050, China
,
C.-C. Zou Key Laboratory of Bioactive Substance and Resources Utilisation of Chinese Herbal Medicine (Peking Union Medical College), Ministry of Education, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Sciences, Beijing, 100050, China
,
L. Zhou Key Laboratory of Bioactive Substance and Resources Utilisation of Chinese Herbal Medicine (Peking Union Medical College), Ministry of Education, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Sciences, Beijing, 100050, China
,
P.-S. Lei Key Laboratory of Bioactive Substance and Resources Utilisation of Chinese Herbal Medicine (Peking Union Medical College), Ministry of Education, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Sciences, Beijing, 100050, ChinaCorrespondence[email protected]
&
D.-Q. Yu Key Laboratory of Bioactive Substance and Resources Utilisation of Chinese Herbal Medicine (Peking Union Medical College), Ministry of Education, Institute of Materia Medica, Peking Union Medical College and Chinese Academy of Medical Sciences, Beijing, 100050, China
Pages 689-696 | Received 15 Apr 2005, Accepted 07 Jun 2005, Published online: 06 Dec 2006
 
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Abstract

Three well-known natural diosgenyl glycosides which have the same sugar chains but different sequence, ophipogonin C′, polyphillin C and prosapogenin B, were synthesised by a facile approach. A method using the levulinyl group as a protecting group to selectively mask the C3–OH of diosgenyl 4,6-O-benzylidene-β-d-glucopyranoside is described.

Acknowledgements

Financial support of this research by the National Natural Science Foundation of China (NSFC 20372085) is gratefully acknowledged by the authors.

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