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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 178, 2003 - Issue 8
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Original Articles

Microwave Induced Reaction of Dialkyl 2-(1-Acetyl-2-Oxopropyl)-3-(triphenylphosphoranylidene) Succinates with Ninhydrin in the Presence of Magnesium Sulfate in Solvent-Free Conditions

Ali Ramazani Zanjan University, Zanjan, Iran
Pages 1839-1844 | Published online: 27 Oct 2010
 
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Abstract

Microwave catalyzed one-pot stereoselective synthesis of dialkyl 1,1-diacetyl-8 a -hydroxy-8-oxo-1,2,8,8 a -tetrahydrocyclopenta[ a ]indene-2,3-carboxylates in fairly high yields by the reaction of dialkyl 2-(1-acetyl-2-oxopropyl)-3-(triphenylphosphoranylidene) succinates and ninhydrin in the presence of MgSO 4 in solvent-free conditions.

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