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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 179, 2004 - Issue 4-5
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Original Articles

CLEAVAGE OF cyclo-(tBuSb)4 WITH Li, Na OR K AND FORMATION OF Sb73 − BY REACTIONS OF PRIMARY STIBINES WITH BuLi OR K

Hans J. Breunig Universität Bremen, Germany
&
Mihaiela E. Ghesner Universität Bremen, Germany
Pages 971-972 | Received 01 Aug 2003, Accepted 01 Oct 2003, Published online: 12 Aug 2010
 
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Abstract

Novel reactions of cyclo-(tBuSb) 4 and RSbH2 (R═C6 H 5 , 2,4,6-(CH3)3 C6 H2 or [(CH3)3Si]2CH) with alkali metals or n-BuLi are described.

We thank Dr. Enno Lork for the supervision of the x-ray structure analyses and the Deutsche Forschungsgemeinschaft for financial support.

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